Search results for "pressurized liquid extraction"

showing 10 items of 10 documents

Analytical strategies to determine quinolone residues in food and the environment

2007

23 páginas, 5 figuras, 5 tablas.

AnalyteQuinoloneSolvent extractionEnvironmental analysismedicine.drug_classPLELCFluorescence spectrometryLiquid chromatographyEnvironmentAnalytical ChemistryCapillary electrophoresisCapillary electrophoresismedicineSample preparationSolid phase extractionSpectroscopySESolid-phase extractionChromatographyMass spectrometryChemistryExtraction (chemistry)MSQuinoloneCEFoodPressurized liquid extractionBiochemical engineeringSPE
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Salmon (Salmo salar) side streams as a bioresource to obtain potential antioxidant peptides after applying pressurized liquid extraction (PLE)

2021

The pressurized liquid extraction (PLE) technique was used to obtain protein extracts with antioxidant capacity from salmon muscle remains, heads, viscera, skin, and tailfins. A protein recovery percentage ≈28% was obtained for all samples except for viscera, which was ≈92%. These values represented an increase of 1.5–4.8-fold compared to stirring extraction (control). Different SDS-PAGE profiles in control and PLE extracts revealed that extraction conditions affected the protein molecular weight distribution of the obtained extracts. Both TEAC (Trolox equivalent antioxidant capacity) and ORAC (oxygen radical antioxidant capacity) assays showed an outstanding antioxidant activity for viscer…

AntioxidantQH301-705.5Electrospray ionizationmedicine.medical_treatmentSalmo salarTrolox equivalent antioxidant capacityPharmaceutical ScienceAquacultureantioxidant capacityMass spectrometry01 natural sciencesAntioxidantsChemistry Techniques AnalyticalMass SpectrometryArticle0404 agricultural biotechnologyMetals HeavymycotoxinsDrug Discoverypressurized liquid extractionPressuremedicineAnimalsFish Proteins DietarySalmoBiology (General)heavy metalsPharmacology Toxicology and Pharmaceutics (miscellaneous)Polyacrylamide gel electrophoresischemistry.chemical_classificationChromatographybiologyChemistryside streams010401 analytical chemistryExtraction (chemistry)Computational Biologysalmon04 agricultural and veterinary sciencesbiology.organism_classification040401 food science0104 chemical sciencesAmino acidMolecular WeightpeptidesElectrophoresis Polyacrylamide GelproteinChromatography LiquidSDS-PAGEMarine Drugs
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Pulsed electric fields (PEF), pressurized liquid extraction (PLE) and combined PEF + PLE process evaluation: Effects on Spirulina microstructure, bio…

2022

This study aims at evaluating the impact of different processes-pulsed electric fields (PEF), pressurized liquid extraction (PLE) and a multistep process combining PEF + PLE on the yield of antioxidant compounds (protein, polyphenols, chlorophyll a, chlorophyll b, and carotenoids) from Spirulina. Firstly, the effects of PEF or PLE treatment on the extraction yield of Spirulina biomolecules were evaluated. To further increase the extraction yield, PEF + PLE was used, as an innovative extraction approach. The results showed that PEF + PLE greatly improved the extraction yield compared with the PEF or PLE treatments alone. Compared with Folch extraction (conventional control technique), PEF + …

BiomoleculesTriple TOF-LC-MS-MSPhenolic profileGeneral Chemistryrespiratory systemPulsed electric fields (PEF)Pressurized liquid extraction (PLE)Industrial and Manufacturing EngineeringAntioxidantsrespiratory tract diseasesimmune system diseasesAlguesMicroalgaeCell structureFood Sciencecirculatory and respiratory physiologyInnovative Food Science & Emerging Technologies
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Pressurized liquid extraction of organic contaminants in environmental and food samples

2015

Pressurized liquid extraction (PLE) is an automated technique that uses elevated temperature and pressure to achieve exhaustive extraction from solid matrices, so reducing solvent consumption and enhancing sample throughput when compared with traditional procedures. Hence, it can be considered an environment-friendly technique, generating small volumes of waste and reducing costs and time. This review focuses on application of this green technique to the analysis of organic contaminants in food and environmental matrices for monitoring purposes. We examine fundamentals and key aspects of the development of a PLE method, including pressurized hot-water extraction, together with some relevant…

ChromatographyPressurized fluid extractionChemistrybusiness.industryAssisted solvent extractionExtraction (chemistry)Supercritical fluid extractionContaminationEnvironmentAutomated techniqueSupercritical fluid extractionAnalytical ChemistryPressurized hot-water extractionIn-cell clean-upTemperature and pressureSoxhlet extractionFoodPressurized liquid extractionMicrowave-assisted extractionSolid phase extractionProcess engineeringbusinessSpectroscopyTrAC - Trends in Analytical Chemistry 71: 55-64 (2015)
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Development of Antioxidant Protein Extracts from Gilthead Sea Bream (Sparus aurata) Side Streams Assisted by Pressurized Liquid Extraction (PLE)

2021

The pressurized liquid extraction (PLE) technique was used, for the first time, to obtain protein extracts with antioxidant activity from side streams (muscle, heads, viscera, skin, and tailfins) of gilthead sea bream (Sparus aurata) in order to give added value to these underutilized matrices. Extraction conditions previously optimized for sea bass (Dicentrarchus labrax) side streams were applied. Protein recovery percentages were 22% (muscle), 33% (heads), 78% (viscera), 24% (skin), and 26% (tailfins), which represented an increase of 1.2–4.5-fold compared to control samples (extraction by stirring). The SDS-PAGE profiles revealed that PLE-assisted extraction influenced protein molecular …

Fish ProteinsSpectrometry Mass Electrospray IonizationAntioxidantOxygen radical absorbance capacityFood HandlingElectrospray ionizationmedicine.medical_treatmentLiquid-Liquid ExtractionTrolox equivalent antioxidant capacityPharmaceutical Scienceantioxidant capacity01 natural sciencesAntioxidantsArticle0404 agricultural biotechnologymycotoxinsDrug Discoverypressurized liquid extractionmedicinePressuregilthead sea breamAnimalsSea bassheavy metalsPharmacology Toxicology and Pharmaceutics (miscellaneous)Inductively coupled plasma mass spectrometrylcsh:QH301-705.5Chromatography High Pressure LiquidWaste ProductsChromatographyOxygen Radical Absorbance CapacitybiologyChemistryside streams010401 analytical chemistryExtraction (chemistry)04 agricultural and veterinary sciencesbiology.organism_classification040401 food scienceSea Bream0104 chemical sciencesMolecular Weightlcsh:Biology (General)MetalsDicentrarchusElectrophoresis Polyacrylamide GelproteinSDS-PAGEMarine Drugs
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An Integrated Approach for the Valorization of Sea Bass (Dicentrarchus labrax) Side Streams: Evaluation of Contaminants and Development of Antioxidan…

2021

In this study, the presence of As, Hg, Cd, Pb, and mycotoxins in sea bass side streams (muscle, head, viscera, skin, and tailfin) was evaluated as a preliminary step to assess the effect of an innovative extraction technique (Pressurized Liquid Extraction

Muscle tissueHealth (social science)Plant Scienceantioxidant capacitylcsh:Chemical technology01 natural sciencesHealth Professions (miscellaneous)MicrobiologyArticleCommercial fish feedchemistry.chemical_compound0404 agricultural biotechnologymycotoxinspressurized liquid extractionmedicinelcsh:TP1-118514. Life underwaterSea bassMycotoxinheavy metalsPolyacrylamide gel electrophoresisChromatographybiologyside streams010401 analytical chemistryExtraction (chemistry)04 agricultural and veterinary sciencesContaminationbiology.organism_classification040401 food science0104 chemical sciencesbody regionsmedicine.anatomical_structurechemistryDicentrarchusproteinsea bassFood ScienceSDS-PAGEFoods
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Pressurized liquid extraction coupled to liquid chromatography for the analysis of ochratoxin A in breakfast and infants cereals from Morocco

2010

Abstract A sensitive and reliable method using pressurized liquid extraction (PLE) and liquid chromatography (LC) has been developed for the analysis of ochratoxin A (OTA) in breakfast and infants cereals. Influence of several extraction solvents that affect PLE efficiency was studied. The selected PLE operating method was: 10 g of sample was packed into 22 ml stainless-steel cell and OTA was extracted with acetonitrile/water (80:20) at 40 °C, 34 atm in one cycle of 5 min at 60% flush. The mean recovery of OTA was 82 ± 4 at fortification level of 3 ng/g OTA. The limit of quantification (LOQ) of OTA was 0.25 ng/g. The proposed method was successfully applied to the analysis of 68 samples of …

Ochratoxin ADetection limitChromatographyMaximum levelLCExtraction (chemistry)Ochratoxin AContaminationPressurized liquid extraction (PLE)chemistry.chemical_compoundchemistryBreakfast cereals; Infant cereals; LC; Ochratoxin A; Pressurized liquid extraction (PLE)Infant cerealsFood scienceFood ScienceBiotechnologyFood contaminantBreakfast cereals
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Evaluation of biological properties of extracts obtained from marine biomass assisted by pulsed electric fields (PEF) and pressurized liquid extracti…

2022

Teniendo en cuenta el gran interés por la biodiversidad, los recursos marinos representan una fuente importante de compuestos de alto valor añadido como proteínas y péptidos bioactivos, lípidos y ácido grados vitaminas, minerales y compuestos bioactivos, etc. Los residuos y subproductos del pescado como cabeza, vísceras y piel, entre otros, se descartan o no se utilizan de manera efectiva durante el procesamiento de los alimentos, lo que resulta en un gran desperdicio de recursos, sin embargo, son una gran fuente de compuestos con alto valor añadido y que pueden tener un potencial uso considerable en las industrias alimentaria, farmacéutica, cosmética y otras, existiendo, por lo tanto, un i…

bioactive compoundspulsed electric fieldsmicroalgaepressurized liquid extractionUNESCO::CIENCIAS DE LA VIDA:CIENCIAS AGRARIAS [UNESCO]fish side streams:CIENCIAS DE LA VIDA [UNESCO]UNESCO::CIENCIAS AGRARIAS
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Green extraction approach for the recovery of polyphenols from Croatian olive leaves (Olea europea)

2017

Abstract Pressurized liquid extraction (PLE) is shown as an innovative green technology for the effective extraction of the various phytochemicals from food by-products, therefore the aims of this study were to evaluate the application of PLE to engineer green extracts of Croatian olive leaves ( Olea europaea , cv. Oblica) for potential industrial production (functional foods/pharmaceuticals). PLE was conducted under various cycle numbers (1, 2), temperature (60, 80, 100 °C) and static times (5, 10, 15 min). Obtained extracts were characterized in terms of: (i) total polyphenols (TP); (ii) total flavonoids (TF); hydroxycinnamic acids (HCA); and (iv) flavonols (FLA). Response surface methodo…

chemistry.chemical_classificationOblica olive leaves ; Green extraction ; Pressurized liquid extraction ; Total polyphenols ; Flavonoids ; Hydroxycinnamic acidsChromatographybiologyGeneral Chemical EngineeringExtraction (chemistry)04 agricultural and veterinary sciencesbiology.organism_classification040401 food scienceBiochemistry0404 agricultural biotechnologyFlavonolschemistryOleaPolyphenolResponse surface methodologyFood ScienceBiotechnologyFood and Bioproducts Processing
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Innovative extraction and separation technologies to improve the recovery of microalgae nutrients and bioactive compounds with potential beneficial e…

2023

Las microalgas son ricas en una gran variedad de compuestos bioactivos, que incluyen proteínas, polifenoles, polisacáridos, pigmentos, minerales, vitaminas, etc., que pueden utilizarse o separarse directamente para obtener componentes de mayor valor. La extracción y la separación son pasos clave en la obtención y posterior procesamiento de los productos relacionados con las microalgas, representando las tecnologías innovadoras de procesado una estrategia innovadora y eficiente para mejorar la calidad de estos productos. Actualmente, las microalgas y sus compuestos (nutrientes, compuestos bioactivos, etc.) se utilizan como alimento y también con finalidades desde el punto de vista de salud, …

electrical pulsesbioactive compoundsnutrientsmicroalgaepressurized liquid extractionhealthUNESCO::CIENCIAS TECNOLÓGICAS::Tecnología de los alimentos
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